Search

제품안내 이온분석기기 전문 기업 (주)제이엘사이언스

    컬럼 (Column)

    Anions

    Metrosep A Supp 4 - 250/4.0

    The Metrosep A Supp 4 - 250/4.0 is an extremely robust column with very good separation properties. The separation phase is comprised of polyvinyl alcohol particles with quaternary ammonium groups and a diameter of 9 µm. This structure guarantees great stability and a greater tolerance to very small particles which could pass through the integrated filter pad. The Metrosep A Supp 4 - 250/4.0 has a medium ion exchange capacity; sulfate elutes after 12.5 minutes. The number of plates which can be achieved with this separation column is higher than those on the Metrosep Anion Dual 2 - 75/4.6. The A Supp 4 - 250/4.0 is particularly suitable for all routine tasks in water analysis.

    The Metrosep A Supp 4 - 250/4.0 is an extremely robust column with very good separation properties. The separation phase is comprised of polyvinyl alcohol particles with quaternary ammonium groups and a diameter of 9 µm. This structure guarantees great stability and a greater tolerance to very small particles which could pass through the integrated filter pad. The Metrosep A Supp 4 - 250/4.0 has a medium ion exchange capacity; sulfate elutes after 12.5 minutes. The number of plates which can be achieved with this separation column is higher than those on the Metrosep Anion Dual 2 - 75/4.6. The A Supp 4 - 250/4.0 is particularly suitable for all routine tasks in water analysis. Its universal applicability makes it the standard column for the 883 Basic IC plus.

    To protect the IC separation column – even though it is not particularly sensitive to contamination – we recommend the use of the Metrosep A Supp 4/5 Guard/4.0 or the A Supp 4/5 S-Guard/4.0.

     

    Column dimensions (mm)250 x 4.0
    Max. pressure12 MPa
    Maximum flow2.0 mL/min
    Standard flow1.0 mL/min
    Housing materialPEEK
    Carrier materialPolyvinyl alcohol with quarternary ammonium groups
    Particle size (µm)9
    Column type1
    pH range3...12
    StorageIn the eluent
    Weight0.28
    Regeneration

    Contamination with hydrophilic ions:

    a) Rinse with ultrapure water (15 min at 0.5 mL/min)
    b) Rinse with 10x concentrated eluent (60 min at 0.5 mL/min)
    c) Rinse with ultrapure water (15 min at 0.5 mL/min)
    d) Rinse with eluent (60 min at 0.5 mL/min)

    Contamination with lipophilic ions:

    a) Rinse with ultrapure water (15 min at 0.5 mL/min)
    b) Rinse with 5% acetonitrile (10 min at 0.5 mL/min)
    c) Rinse with 100% acetonitrile (60 min at 0.5 mL/min)
    d) Rinse with 50% acetonitrile (10 min at 0.5 mL/min)
    e) Rinse with ultrapure water (30 min at 0.5 mL/min)
    f) Rinse with eluent (60 min at 0.5 mL/min)

    Application range

    Applications

    • Standard anions
    • Water analysis
    • Difficult matrices
    • Critical samples
    • Iodide
    Capacity71 (µmol Cl)
    Organic modifier

    0 - 100%

    Eluents

    Phthalate eluent (standard eluent)
    Without chemical suppression

    Phthalic acid: 5.0 mmol/L; 1,660 mg/2 L
    Acetone: 2.0%; 40 mL/2 L
    TRIS: pH = 4.4

    Carbonate eluent (standard eluent)
    With chemical suppression

    Sodium bicarbonate: 1.7 mmol/L; 286 mg/2 L
    Sodium carbonate: 1.8 mmol/L; 382 mg/2 L

    Carbonate eluent, modified

    Sodium bicarbonate: 4.0 mmol/L; 672 mg/2 L
    Sodium carbonate: 1.0 mmol/L; 212 mg/2 L

    Options
    6.1006.500Metrosep A SUPP 4/5 Guard/4.0
    6.1006.540Metrosep A Supp 4/5 S-Guard/4.0